反应条件
1: LDA / tetrahydrofuran / 0.5 h / -40 °C
2: 81 percent / tetrahydrofuran / 1) -40 deg C, 2) 30 min, reflux
3: 100 percent / LiAlH4 / tetrahydrofuran / 0 °C
4: 69 percent / Br2 / CCl4 / 1) r.t., 2) 150 deg C, 1,5 h
View Scheme
参考文献
Kauffmann, Thomas; Fischer, Heinz; Woltermann, Annegret
Chemische Berichte, 1982 , vol. 115, # 2 p. 645 - 653
