2-氨基-4'-氯二苯甲酮合成路线 （共 30 条）
反应条件
1: dodecanesulphonic acid sodium salt / water / 0.5 h / 20 °C 2: palladium diacetate; trifluoroacetic acid; tert.-butylhydroperoxide / water / 24 h / 20 °C 3: hydrogenchloride / water / 3 h / 125 °C View Scheme
参考文献
Szabo, Fruzsina; Simko, Daniel; Novak, Zoltan
RSC Advances, 2014 , vol. 4, # 8 p. 3883 - 3886
反应条件
aluminium trichloride; phosphorus pentachloride
参考文献
Hall,J.H. et al.
Journal of the American Chemical Society, 1972 , vol. 94, p. 4952 - 4958
反应条件
1: AlCl3 / 4 h / 80 - 90 °C 2: conc. H2SO4 / 0.25 h / 120 °C View Scheme
参考文献
Hu, Wenhui; Guo, Zongru; Chu, Fengming; Bai, Aiping; Yi, Xiang; Cheng, Guifang; Li, Jing
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1153 - 1160
反应条件
ethanol; calcium chloride; zinc
参考文献
Tanasescu; Silberg
Bulletin de la Societe Chimique de France, 1936 , vol. <5> 3, p. 2383
反应条件
hydrogenchloride; magnesium 1) Et2O, reflux, 30 min 2) Et2O, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Fryer; Gu; Wang
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 7 p. 1661 - 1669
参考文献
Bolton, Roger; Mguni, Raphael S.; Williams, Gareth H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 405 - 408
反应条件
potassium carbonate T=80°C; Suzuki Coupling; P=760.051 Torr; 12 h; Catalytic behavior;
参考文献
Niu, Jianrui; Liu, Mengmeng; Wang, Peng; Long, Yu; Xie, Miao; Li, Rong; Ma, Jiantai
New Journal of Chemistry, 2014 , vol. 38, # 4 p. 1471 - 1476
参考文献
Wegerhoff
Justus Liebigs Annalen der Chemie, 1889 , vol. 252, p. 36
参考文献
Hantzsch
Chemische Berichte, 1891 , vol. 24, p. 41
参考文献
Wegerhoff
Justus Liebigs Annalen der Chemie, 1889 , vol. 252, p. 36
