1,3,5,7,2,4,6,8-四硫杂四氮杂环辛四烯合成路线 (共 142 条)
反应条件
in neat (no solvent) react. of PCl3 with N4S4;; recrystn. from CHCl3 at -55 °C; washing with CCl4;;
参考文献
Naturwissenschaften, , vol. 48, p. 25 - 25
P: MVol.C, 233, page 533 - 535
反应条件
in benzene addn. of PCl3 to a soln. of S4N4 in C6H6 containing SOCl2; formation of a brown main product and crystals of (PNCl2)3;;
参考文献
Gmelin Handbook: P: MVol.C, 184, page 424 - 427
反应条件
in benzene formation of phosphorus nitride dichlorides with a large amount of (NPCl2)3 as by-products by addn. of PCl3 to a soln. of S4N4 in C6H6 containing SOCl2;;
参考文献
Gmelin Handbook: P: MVol.C, 240, page 549 - 551
反应条件
in tetrachloromethane boiling in CCl4 for several hours;;
参考文献
Gmelin Handbook: Ag: MVol.B1, 5.15.3.4, page 312 - 313
反应条件
in tetrachloromethane addition of AgF2 to a solution of S4N4 in CCl4; formation of SNF and SN2F2 on boiling;; evaporation;;
参考文献
Gmelin Handbook: Ag: MVol.B1, 5.15.3.4, page 312 - 313
反应条件
water in water 24 h shaking, cold water;;
参考文献
Gmelin Handbook: S: MVol.B3, 7, page 1545 - 1547
反应条件
hydrogenchloride in hydrogenchloride hydrolysis;;
参考文献
Gmelin Handbook: S: MVol.B3, 7, page 1545 - 1547
反应条件
acid in benzene acid hydrolysis of S4N4; small amt. of H2S;
参考文献
Nair, C. G. R.; Murthy, A. R. V.
Journal of Inorganic and Nuclear Chemistry, 1963 , vol. 25, p. 453 - 459
Full Text View citing articles Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.4.4, page 22 - 22
参考文献
Ruff, O.; Geisel, E.
Ber., 1904 , vol. 37, p. 1573 - 1595
Full Text Show Details
Gmelin Handbook: S: MVol.B3, 7, page 1545 - 1547
参考文献
Gmelin Handbook: Sn: Org.Verb.1, 1, page 17 - 35