1,3,5,7,2,4,6,8-四硫杂四氮杂环辛四烯合成路线 （共 142 条）
反应条件
water; tin(ll) chloride in benzene byproducts: HCl, ClSn(OH)3*H2O; reduction;;
参考文献
Meuwsen, A.
Ber., 1929 , vol. 62, p. 1959 - 1969
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Woelbling, H.
Z. Anorg. Chem., 1908 , vol. 57, p. 281 - 289
反应条件
in tetrachloromethane byproducts: S8; reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products;; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
in neat (no solvent)
参考文献
Gmelin Handbook: S: MVol.B3, 153, page 1854 - 1856
反应条件
in tetrachloromethane reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
in tetrachloromethane reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
chlorine in chloroform introduction of Cl2 into chloroformic suspension;;
参考文献
Demarcay, E.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1880 , vol. 91, p. 854 - 856
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Gmelin Handbook: S: MVol.B3, 8, page 1547 - 1549
反应条件
in tetrachloromethane introduction of Cl2 into soln. of S4N4 in CCl4;;
参考文献
Glemser, O.; Perl, H.
Naturwissenschaften, 1961 , vol. 48, p. 620 - 620
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Gmelin Handbook: S: MVol.B3, 150, page 1847 - 1849
反应条件
in tetrachloromethane boiling in CCl4 for several hours;;
参考文献
Gmelin Handbook: Ag: MVol.B1, 5.15.3.4, page 312 - 313
反应条件
in thionyl chloride introduction of SO2 into S4N4 dild. in SOCl2 for two hours;; pptn. on cooling;;
参考文献
Goehring, M.; Heinke, J.
Z. Anorg. Chem., 1953 , vol. 272, p. 297 - 302
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Gmelin Handbook: S: MVol.B3, 16, page 1562 - 1564
参考文献
Goehring, M.; Heinke, J.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1955 , vol. 278, p. 53 - 57
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Gmelin Handbook: S: SVol.3, 2.1.8.9.6.3, page 198 - 199
