1,3,5,7,2,4,6,8-四硫杂四氮杂环辛四烯合成路线 （共 142 条）
反应条件
water in gas
excess of SO2, 50-80°C, the solid product hydrolysed by water;
参考文献
Goehring, M.; Kaloumenos, H.-W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1950 , vol. 263, p. 137 - 144
Full Text Show Details
Gmelin Handbook: S: SVol.3, 2.1.8.9.4.1, page 188 - 190
反应条件
water in water
hydrolysis by hot water;; further uncharacterized by-product containing 75percent S and oxygen;;
参考文献
Gmelin Handbook: S: MVol.B3, 155, page 1858 - 1860
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Rochus, V.
Diss. Berlin 1906, S. 30
反应条件
H2O in carbon disulfide
addn. of water to soln. in CS2;;
参考文献
Gmelin Handbook: S: MVol.B3, 152, page 1851 - 1854
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Rochus, V.
Diss. Berlin 1906, S. 25
反应条件
in neat (no solvent)
heated slowly to 125°C, 10 min; within 18 h S4N4 sublimed off under vac. at 70-80°C;
参考文献
Roesky, H. W.; Anhaus, J.; Sheldrick, W. S.
Inorganic Chemistry, 1984 , vol. 23, p. 75 - 79
反应条件
in hexane
Kinetics; other Radiation; soln. of S4N4 in hexane subjected to laser flash photolysis (low intensity) at 266 or 308 nm at ca. 295 K; monitored by UV-vis spectra;
参考文献
Pritchina, Elena A.; Terpilovskaya, Daria S.; Tsentalovich, Yuri P.; Platz, Matthew S.; Gritsan, Nina P.
Inorganic Chemistry, 2012 , vol. 51, # 8 p. 4747 - 4755
反应条件
water in gas
excess of SO2, 40-50°C, the solid product hydrolysed by water;
参考文献
Goehring, M.; Kaloumenos, H.-W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1950 , vol. 263, p. 137 - 144
Full Text Show Details
Gmelin Handbook: S: SVol.3, 2.1.8.9.4.1, page 188 - 190
反应条件
in toluene
liquid ammonia dropped into cooled SCl2 in toluene until pptn.; (further diluents: CCl4, CHCl3, benzene, ethylether, dry sand); evapn. of NH3; filtration from toluene; removal of NH4Cl (water); mixture of S4N4 and sulfur obtained;;
参考文献
Gmelin Handbook: S: MVol.B3, 5, page 1540 - 1543
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Fernelius, W. C.
Patent: US2207791 , 1940 ;
C. II, 1940 , p. 3694
反应条件
in not given
activated nitrogen;;
参考文献
Strutt, R. J.
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1913 , vol. 88, p. 539 - 549
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Gmelin Handbook: S: MVol.B3, 4, page 1537 - 1540
参考文献
Andreocci, A.
Z. Anorg. Chem., 1897 , vol. 14, p. 246 - 250
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Andreocci, A.
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1896 , vol. 5, # II p. 254 - 258
Full Text Show Details
Gmelin Handbook: S: MVol.B3, 4, page 1537 - 1540
反应条件
in neat (no solvent)
introduction of dry ammonia (water bath);; extraction by boiling CS2;;
参考文献
Gmelin Handbook: S: MVol.B3, 4, page 1537 - 1540
