2-环丙甲基氨基-5-氯二苯甲酮合成路线 （共 5 条）
反应条件
triethylamine in benzene
2 h; Ambient temperature;
参考文献
Yamamoto
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 8 p. 2135 - 2156
反应条件
in methanol; chloroform
T=45 - 50°C; P=76000.1 Torr; 31 h;
参考文献
Cinellu, Maria Agostina; Gladiali, Serafino; Minghetti, Giovanni; Stoccoro, Sergio; Demartin, Francesco
Journal of Organometallic Chemistry, 1991 , vol. 401, # 3 p. 371 - 384
反应条件
in chloroform
T=45 - 50°C; P=76000.1 Torr; 31 h; Title compound not separated from byproducts;
参考文献
Cinellu, Maria Agostina; Gladiali, Serafino; Minghetti, Giovanni; Stoccoro, Sergio; Demartin, Francesco
Journal of Organometallic Chemistry, 1991 , vol. 401, # 3 p. 371 - 384
反应条件
hydrogenchloride
multistep reaction: acid hydrolysis, photolysis;
参考文献
Schutz; Fitz
Arzneimittel-Forschung/Drug Research, 1982 , vol. 32, # 3 p. 177 - 183
反应条件
hydrogenchloride
multistep reaction: acid hydrolysis, photolysis;
参考文献
Schutz; Fitz
Arzneimittel-Forschung/Drug Research, 1982 , vol. 32, # 3 p. 177 - 183
