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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
28995-88-2
合成路线
（共 49 条）
→
反应条件
70312-74-2
反应条件
CuCN in tetrahydrofuran; dichloromethane T=-20°C; 0.5 h;
参考文献
Xie, Meihua; Huang, Xian
Synlett, 2003 , # 4 p. 477 - 480
696-62-8
4-碘苯甲醚
+
28995-88-2
→
反应条件
7380-78-1
1-甲氧基-4-苯基乙炔苯
反应条件
1: para-iodoanisole With n-butyllithium in diethyl ether; hexane Inert atmosphereCooling; 2: 1-(4'-methylphenylsulfonyl)-2-phenylethyne in diethyl ether; hexane 0.25 h; Inert atmosphere; regioselective reaction;
参考文献
Garcia Ruano, Jose Luis; Aleman, Jose; Marzo, Leyre; Alvarado, Cuauhtemoc; Tortosa, Mariola; Diaz-Tendero, Sergio; Fraile, Alberto
Chemistry - A European Journal, 2012 , vol. 18, # 27 p. 8414 - 8422
14774-77-7
+
28995-88-2
→
反应条件
7380-78-1
1-甲氧基-4-苯基乙炔苯
反应条件
in tetrahydrofuran T=-78°C; 0.0833333 h;
参考文献
Marzo, Leyre; Aleman, Jose; Garcia Ruano, Jose Luis
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 4 p. 403 - 407
→
反应条件
81763-73-7
反应条件
in tetrahydrofuran; dichloromethane T=-20°C; 0.0833333 h;
参考文献
Huang, Xian; Xie, Meihua
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 8895 - 8900
594-19-4
叔丁基锂
+
28995-88-2
→
反应条件
4250-82-2
(3,3-二甲基-1-丁炔)-苯
反应条件
in tetrahydrofuran; pentane T=-78°C; Inert atmosphere; regioselective reaction;
参考文献
Marzo, Leyre; Aleman, Jose; Garcia Ruano, Jose Luis
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 4 p. 403 - 407
188290-36-0
+
28995-88-2
→
反应条件
4805-17-8
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexane T=0°C; Inert atmosphere; 2: 1-(4'-methylphenylsulfonyl)-2-phenylethyne in tetrahydrofuran; pentane T=-78°C; 0.25 h; Inert atmosphere; regioselective reaction;
参考文献
Garcia Ruano, Jose Luis; Aleman, Jose; Marzo, Leyre; Alvarado, Cuauhtemoc; Tortosa, Mariola; Diaz-Tendero, Sergio; Fraile, Alberto
Chemistry - A European Journal, 2012 , vol. 18, # 27 p. 8414 - 8422
917-92-0
3,3-二甲基-1-丁炔
+
28995-88-2
→
反应条件
62217-46-3
反应条件
1: 3,3-dimethylbut-1-yne With ethylmagnesium bromide in tetrahydrofuran T=25°C; 0.5 h; 2: 1-(4'-methylphenylsulfonyl)-2-phenylethyne With bis(acetylacetonate)nickel(II) in tetrahydrofuran T=25°C;
参考文献
Fang, Kuang; Xie, Meihua; Zhang, Zhannan; Ning, Peng; Shu, Guanying
Tetrahedron Letters, 2013 , vol. 54, # 29 p. 3819 - 3821
100-66-3
苯甲醚
+
28995-88-2
→
反应条件
41398-67-8
1-甲氧基-2-苯基乙炔-苯
反应条件
1: methoxybenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Inert atmosphere; 2: 1-(4'-methylphenylsulfonyl)-2-phenylethyne in tetrahydrofuran; hexane T=-78°C; 0.0833333 h; Inert atmosphere; regioselective reaction;
参考文献
Garcia Ruano, Jose Luis; Aleman, Jose; Marzo, Leyre; Alvarado, Cuauhtemoc; Tortosa, Mariola; Diaz-Tendero, Sergio; Fraile, Alberto
Chemistry - A European Journal, 2012 , vol. 18, # 27 p. 8414 - 8422
591-51-5
苯基锂
+
28995-88-2
→
反应条件
501-65-5
二苯基乙炔
反应条件
in tetrahydrofuran; anhydrous butyl ether T=-78°C; Inert atmosphere; regioselective reaction;
参考文献
Garcia Ruano, Jose Luis; Aleman, Jose; Marzo, Leyre; Alvarado, Cuauhtemoc; Tortosa, Mariola; Diaz-Tendero, Sergio; Fraile, Alberto
Chemistry - A European Journal, 2012 , vol. 18, # 27 p. 8414 - 8422
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