N-乙酰-DL-苯丙氨酸合成路线 （共 69 条）
反应条件
T=150°C; microwave irradiation;
参考文献
Wang, Xiao-Jian; Yang, Qian; Liu, Fei; You, Qi-Dong
Synthetic Communications, 2008 , vol. 38, # 7 p. 1028 - 1035
反应条件
1.1: Raney nickel / methanol / 20 °C 1.2: 50 - 64 °C 2.1: methanol / 20 °C View Scheme
参考文献
Yang, Yihua; Liu, Shouxin; Li, Junzhang; Tian, Xia; Zhen, Xiaoli; Han, Jianrong
Synthetic Communications, 2012 , vol. 42, # 17 p. 2540 - 2554
反应条件
water; hydroxide T=25°C; different reaction conditions; solvent effect; Rate constantProduct distribution;
参考文献
Daffe, Viviane; Fastrez, Jacques
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 783 - 788
反应条件
water; triethylamine in ethylene glycol dimethyl ether Yield given. Yields of byproduct given;
参考文献
Lyubeznova, M. R.; Karpeiskaya, E. I.; Klabunovskii, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.1 p. 720 - 726
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 811 - 818
反应条件
triethylamine in tert-butyl alcohol Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lyubeznova, M. R.; Karpeiskaya, E. I.; Klabunovskii, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.1 p. 720 - 726
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 811 - 818
参考文献
Bergmann; Stern
Chemische Berichte, 1930 , vol. 63, p. 438
反应条件
styrene and divinylbenzene; hydrogen; palladium in ethylene glycol dimethyl ether T=20°C; reductive solvolysis and hydrogenation of products on var. polymeric Pd-catalyst system; Rate constant;
参考文献
Karpeiskaya, I. E.; Godunova, L. F.; Levitina, E. S.; Lyubeznova, M. R.; Klabunovskii, E. I.; et al.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 10.2 p. 2368 - 2380,1858 - 1867
反应条件
T=95 - 120°C; Acetylation; racemization;
参考文献
Kotlova; Timokhina; Chestukhina; Stepanov
Russian Journal of Bioorganic Chemistry, 1999 , vol. 25, # 9 p. 579 - 583
反应条件
acetic acid 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Rosnati, Vittorio; Saba, Antonio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 3/4 p. 149 - 152
参考文献
Andersen, Kenneth K.; Gloster, Daniel F.; Bray, Diana D.; Shoja, Massud; Kjaer, Anders
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 2 p. 317 - 324
