2,2,2-三氯苯乙酮合成路线 （共 148 条）
反应条件
in dichloromethane
T=25°C; other solvents; Rate constant;
参考文献
Druzian, Janice; Zucco, Cesar; Rezende, Marcos Caroli; Nome, Faruk
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4767 - 4771
反应条件
1: PCl5 / 220 °C
2: anhydrous HF / 145 - 155 °C / 14710.2 Torr
View Scheme
参考文献
Simons; Herman
Journal of the American Chemical Society, 1943 , vol. 65, p. 2064
反应条件
thioacetic acid sodium salt in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Romero-Ortega, Moises; Reyes, Horacio; Covarruvias-Zuniga, Adrian; Cruz, Raymundo; Avila-Zarraga, Jose Gustave
Synthesis, 2003 , # 18 p. 2765 - 2767
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent)
T=20 - 25°C; 10 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
1: 70 percent / benzene / 18 h / Ambient temperature
2: 85 percent / 1 percent KOH / ethanol / 16 h / 20 °C
View Scheme
参考文献
Kozlov, E. S.; Dubenko, L. G.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 12 p. 2707 - 2711,2396 - 2399
反应条件
NaOH (buffer pH 8.00); Tween-80 in water
T=25°C; other catalysts: cationic (CTABr and CTACl) and anionic (SDS) surfactants; pH-dependence; Rate constant;
参考文献
Nascimento, Maria da Graca; Lezcano, Maria Ada; Nome, Faruk
Journal of Physical Chemistry, 1992 , vol. 96, # 13 p. 5537 - 5540
反应条件
sodium hydroxide
oder Homologen von Edukt 1;
参考文献
Houben; Fischer
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 123, p. 319
Chemische Berichte, 1933 , vol. 66, p. 341
反应条件
sodium hydroxide in water
T=25°C; different concentrations of the base; KineticsRate constant;
参考文献
Guthrie, J. Peter; Cossar, John
Canadian Journal of Chemistry, 1990 , vol. 68, # 9 p. 1640 - 1642
反应条件
in acetonitrile
T=25°C; Rate constant;
参考文献
Druzian, Janice; Zucco, Cesar; Rezende, Marcos Caroli; Nome, Faruk
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4767 - 4771
反应条件
in n-heptane
T=25°C; other solvents; Rate constant;
参考文献
Druzian, Janice; Zucco, Cesar; Rezende, Marcos Caroli; Nome, Faruk
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4767 - 4771
