2,2,2-三氯苯乙酮合成路线 （共 148 条）
反应条件
isopropylmagnesium chloride in tetrahydrofuran T=-78°C;
参考文献
Rodriguez, Cristina; Borzecka, Wioleta; Sattler, Johann H.; Kroutil, Wolfgang; Lavandera, Ivan; Gotor, Vicente
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 4 p. 673 - 681
参考文献
Meerwein; Schmidt
Justus Liebigs Annalen der Chemie, 1925 , vol. 444, p. 233
参考文献
Meerwein et al.
Journal fuer Praktische Chemie (Leipzig), 1936 , vol. <2> 147, p. 226,239
参考文献
Bergkvist
Svensk Kemisk Tidskrift, 1947 , vol. 59, p. 24,26
参考文献
Meerwein; Schmidt
Justus Liebigs Annalen der Chemie, 1925 , vol. 444, p. 233
反应条件
in methanol 16.5 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 4835 - 4838
反应条件
16.5 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 4835 - 4838
反应条件
hydrazine hydrate in hexane 0.5 h; Ambient temperature;
参考文献
Rebelo, Ricardo Andrade; Rezende, Marcos Caroli; Nome, Faruk; Zucco, Cesar
Synthetic Communications, 1987 , vol. 17, # 14 p. 1741 - 1748
反应条件
potassium tert-butylate 1.) DMSO, 5-10 deg C, 30 min, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Hess, Sonia Corina; Nome, Faruk; Zucco, Cesar; Rezende, Marcos Caroli
Synthetic Communications, 1989 , vol. 19, # 17 p. 3037 - 3046
反应条件
1: cathecolborane / (5S)-2-(n-butyl)-4,4-diphenyl-3,1,2-oxazaborabicyclo<3.3.0>octane / toluene / 12 h / -78 °C 2: NaCNBH3, AIBN, Bu3SnCl / ethanol / Heating View Scheme
参考文献
Corey, E. J.; Helal, Christopher J.
Tetrahedron Letters, 1993 , vol. 34, # 33 p. 5227 - 5230
