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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
Fmoc-甘氨酸
合成路线
（共 81 条）
124-07-2
辛酸
→
反应条件
138531-93-8
Trichogin A IV
反应条件
1: H-L-Lol-2-chlorotrityl resin; fmoc-L-Ile-OH With N-ethyl-N,N-diisopropylamine; HATU 1 h; solid phase reaction; 2: With piperidine in N,N-dimethyl-formamide solid phase reaction; 3: octanoic acid; N-(9-fluorenylmethoxycarbonyl)glycine; N-Fmoc-L-leucine; Fmoc-(α-aminoisobutyric acid)
参考文献
De Zotti, Marta; Biondi, Barbara; Peggion, Cristina; Formaggio, Fernando; Park, Yoonkyung; Hahm, Kyung-Soo; Toniolo, Claudio
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 6 p. 1285 - 1299
29022-11-5
Fmoc-甘氨酸
+
71989-26-9
N-芴甲氧羰基-N'-叔丁氧羰基-L-赖氨酸
+
86123-10-6
Fmoc-D-苯丙氨酸
+
146982-24-3
Fmoc-L-天冬氨酸 4-烯丙酯
→
反应条件
161552-03-0
Cyclic RGDFK peptide
反应条件
1: Fmoc–Asp(OAll)–OH With N-ethyl-N,N-diisopropylamine in dichloromethane 3 h; 2-chlorotrityl chloride polystyrene resin; 2: With piperidine in 1-methyl-pyrrolidin-2-one 0.416667 h; 3: N-(9-fluorenylmethoxycarbonyl)glycine; N-(fluoren-9-ylmethoxycarbonyl)-L-Lys(Nε-Boc); FMOC-D-Phenylalanine; fmoc-L-Arg(Pbf)-OH Further stages;
参考文献
Munch, Henrik K.; Rasmussen, Jakob E.; Popa, Gina; Christensen, Jorn B.; Jensen, Knud J.
Chemical Communications, 2013 , vol. 49, # 19 p. 1936 - 1938
→
反应条件
161552-03-0
Cyclic RGDFK peptide
反应条件
1: Fmoc-Asp(OAll)-Pol 2: N-(9-fluorenylmethoxycarbonyl)glycine 3: N-(fluoren-9-ylmethoxycarbonyl)-L-Lys(Nε-Boc); FMOC-D-Phenylalanine; fmoc-L-Arg(Pbf)-OH Further stages;
参考文献
Waengler, Carmen; Maschauer, Simone; Prante, Olaf; Schaefer, Martin; Schirrmacher, Ralf; Bartenstein, Peter; Eisenhut, Michael; Waengler, Bjoern
ChemBioChem, 2010 , vol. 11, # 15 p. 2168 - 2181
29022-11-5
Fmoc-甘氨酸
→
反应条件
716-94-9
2-氨基-N-2-萘基-乙酰胺
反应条件
piperidine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid 1.) DMF, 2.) CH2Cl2; Yield given. Multistep reaction;
参考文献
Garigipati, Ravi S.
Tetrahedron Letters, 1997 , vol. 38, # 39 p. 6807 - 6810
29022-11-5
Fmoc-甘氨酸
+
116611-64-4
N-芴甲氧羰基-L-组氨酸
→
反应条件
7451-76-5
甘氨酰甘氨酰-L-组氨酸
反应条件
1: Fmoc-(S)-histidine With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine in 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide Automated synthesizersolid phase reaction; 2: With piperidine in 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide 0.216667 h; Automated synthesizersolid phase reaction; 3: N-(9-fluorenylmethoxycarbonyl)glycine Further stages;
参考文献
Stadlbauer, Stefan; Riechers, Alexander; Spaeth, Andreas; Koenig, Burkhard
Chemistry - A European Journal, 2008 , vol. 14, # 8 p. 2536 - 2541
29022-11-5
Fmoc-甘氨酸
→
反应条件
75007-28-2
反应条件
1: With HATU 2: With tri-iso-propylsilane; trifluoroacetic acid T=20°C; 2 h; 3: With piperidine in N,N-dimethyl-formamide
参考文献
Kuriyama, Isoko; Asano, Naoki; Kato, Ikuo; Ikeda, Kyoko; Takemura, Masaharu; Yoshida, Hiromi; Sakaguchi, Kengo; Mizushina, Yoshiyuki
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 2187 - 2196
→
反应条件
79985-48-1
DYNORPHIN A (1-11) AMIDE
反应条件
1: C29H30NO7Pol With piperidine in N,N-dimethyl-formamide 0.333333 h; solid phase reaction; 2: N-(fluoren-9-ylmethoxycarbonyl)-L-Lys(Nε-Boc) With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate in dichloromethane; N,N-dimethyl-formamide 2 h; solid phase reaction; 3: N-(9-fluorenylmethoxycarbonyl)glycine; N-Fmoc-L-leucine; Fmoc–Pro–OH; Fmoc-L-phenylalanine; fmoc-L-Ile-OH; fmoc-O-tert-butyl-L-tyrosine; fmoc-L-Arg(Pbf)-OH Further stages;
参考文献
Patkar, Kshitij A.; Murray, Thomas F.; Aldrich, Jane V.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 21 p. 6814 - 6821
506-68-3
溴化氰
+
29022-11-5
Fmoc-甘氨酸
+
552-89-6
邻硝基苯甲醛
→
反应条件
50608-24-7
反应条件
Multistep reaction;
参考文献
Grover, Rajesh K.; Kesarwani, Amit P.; Srivastava, Gaurav K.; Kundu, Bijoy; Roy, Raja
Tetrahedron, 2005 , vol. 61, # 21 p. 5011 - 5018
29022-11-5
Fmoc-甘氨酸
→
反应条件
611198-15-3
反应条件
1: N-methylmorpholine / tetrahydrofuran / 0.08 h / -10 °C 2: aq. NaN3 / tetrahydrofuran / 0.5 h 3: toluene / 1 h / 90 °C View Scheme
参考文献
Ramesh; Raju; Srinivas; Sureshbabu; Narendra; Vasantha
Journal of Mass Spectrometry, 2010 , vol. 45, # 12 p. 1461 - 1472
29022-11-5
Fmoc-甘氨酸
+
71-36-3
正丁醇
+
99-96-7
对羟基苯甲酸
→
反应条件
51220-55-4
反应条件
Multistep reaction;
参考文献
Basso, Andrea; Evans, Brian; Pegg, Neil; Bradley, Mark
Tetrahedron Letters, 2000 , vol. 41, # 19 p. 3763 - 3767
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