N-(4-氯苯基)-对甲苯磺酰胺合成路线 （共 33 条）
反应条件
1: alcoholic alkali 2: sulfuric acid / 145 °C / Hydrolysis.dann bei 130grad View Scheme
参考文献
Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1847
反应条件
perchloric acid; acetic acid 1 h; Heating;
参考文献
Kudav, D.P.; Samant,S.P.; Hosangadi, B.D.
Synthetic Communications, 1987 , vol. 17, # 10 p. 1185 - 1188
参考文献
Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1847
反应条件
potassium carbonate in water
1 h; RefluxGreen chemistry;
参考文献
Nasrollahzadeh, Mahmoud; Rostami-Vartooni, Akbar; Ehsani, Ali; Moghadam, Majid
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 387, p. 123 - 129
反应条件
in pyridine; acetonitrile
T=20°C; 16 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1174028 A1, 2002 ;
Location in patent: Example 48 ;
反应条件
N-chloro-succinimide; oxygen; copper dichloride in acetonitrile
T=100°C; P=760.051 Torr; 4 h; regioselective reaction;
参考文献
Urones, Beatriz; Martinez, Angel Manu; Rodriguez, Nuria; Arrayas, Ramon Gomez; Carretero, Juan C.
Chemical Communications, 2013 , vol. 49, # 94 p. 11044 - 11046
反应条件
copper(l) chloride in methanol
T=20°C; Chan-Lam Coupling; 2 h;
参考文献
Moon, Soo-Yeon; Nam, Jungsoo; Rathwell, Kris; Kim, Won-Suk
Organic Letters, 2014 , vol. 16, # 2 p. 338 - 341
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
copper(l) iodide; manganese(II) fluoride; potassium hydroxide; N-methyl-2-(methylamino)ethylamine in water
T=60°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Ithnin, Idzham Khalid; Yio, Siew-Hui Trionna; Lin, Zhiyin
European Journal of Organic Chemistry, 2013 , # 3 p. 515 - 524
反应条件
molecular sieve; tris(3,4,5-tribromopyrazol-1-yl)Cu(NCMe)
T=80°C;
参考文献
Fructos, Manuel R.; Trofimenko, Swiatoslaw; Mar Diaz-Requejo; Perez, Pedro J.
Journal of the American Chemical Society, 2006 , vol. 128, # 36 p. 11784 - 11791
