DL-2-氯-2-苯基乙酰氯合成路线 （共 51 条）
反应条件
1: 68 percent / Et3N / hexane / 2.5 h / Heating
2: Zn, acetic acid / H2O / 24 h / Ambient temperature
View Scheme
参考文献
Brady; Shieh
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 5 p. 1337 - 1339
反应条件
1: Et3N / hexane / 2.5 h / Heating
2: Zn, acetic acid / H2O / 24 h / Ambient temperature
View Scheme
参考文献
Brady, William T.; Agho, Michael O.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5337 - 5341
反应条件
1: Et3N / hexane / 2.5 h / Heating
2: Et3N / benzene / Heating
3: 71 percent / NBS, benzoyl peroxide / CCl4 / 18 h / Heating
View Scheme
参考文献
Brady, William T.; Agho, Michael O.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5337 - 5341
反应条件
1: triethylamine / hexane / 2 h / Heating
2: Zn powder, aq. acetic acid / 24 h / Ambient temperature
3: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / chlorobenzene / 18 h / Heating
View Scheme
参考文献
Brady; Shieh
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 5 p. 1337 - 1339
反应条件
1: triethylamine / hexane / 2 h / Heating
2: Zn powder, aq. acetic acid / 24 h / Ambient temperature
3: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / chlorobenzene / 18 h / Heating
View Scheme
参考文献
Brady; Shieh
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 5 p. 1337 - 1339
反应条件
1: carbon disulfide; isopropylamine in neat (no solvent)
T=20°C; 0.0333333 h; Green chemistry;
2: rac-α-chlorophenylacetyl chloride in neat (no solvent)
0.0833333 h; Green chemistry;
参考文献
Nasiri, Farough; Zolali, Amin; Azimian, Zeinab
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 62 - 66
参考文献
Boyle; McKenzie; Mitchell
Chemische Berichte, 1937 , vol. 70, p. 2153,2159
反应条件
Behandeln des erwaermten Reaktionsgemisches mit wss. Schwefelsaeure;
参考文献
Boyle; McKenzie; Mitchell
Chemische Berichte, 1937 , vol. 70, p. 2153,2159
参考文献
Najer,H.; Giudicelli,R.
Bulletin de la Societe Chimique de France, 1961 , p. 1231 - 1238
反应条件
pyridine in toluene
T=55°C; 2 h;
参考文献
KATHOLIEKE UNIVERSITEIT LEUVEN; BARDIOT, Dorothée; CARLENS, Gunter; DALLMEIER, Kai; KAPTEIN, Suzanne; McNAUGHTON, Michael; MARCHAND, Arnaud; NEYTS, Johan; SMETS, Wim
Patent: WO2013/45516 A1, 2013 ;
Location in patent: Page/Page column 128; 132 ;
