2,2-二甲基-1,3-二氧环戊烷合成路线 (共 42 条)
反应条件
1: Addition; 2 h; UV-irradiation; 2: With hydrogenchloride; methanol; water Hydrolysis; 3 h; Heating; Title compound not separated from byproducts;
参考文献
Cirkva, Vladimir; Paleta, Oldrich
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 141 - 156
反应条件
Montmorillonite clay KSF
T=120°C; 0.25 h; Irradiation;
参考文献
Perio, Bertrand; Dozias, Marie-Joelle; Jacquault, Patrick; Hamelin, Jack
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7867 - 7870
反应条件
lt;Pd(H2O)2(Ph2PCH2CH2PPh2)gt;(CF3SO3)2 in dichloromethane
8 h; Ambient temperature;
参考文献
Gorla, Fabrizio; Venanzi, Luigi M.
Helvetica Chimica Acta, 1990 , vol. 73, # 3 p. 690 - 697
反应条件
bromine in tetrachloromethane
T=60 - 70°C;
参考文献
Vershinin; Makayeva; Zorina; Zorin; Rahmankulov
Russian Journal of General Chemistry, 1996 , vol. 66, # 7 p. 1147 - 1149
反应条件
in acetonitrile
1 h; Irradiation; Quantum yieldMechanism;
参考文献
Mella, M.; Fasani, E.; Albini, A.
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3051 - 3057
反应条件
Montmorillonite clay KSF
T=120°C; 0.5 h; Irradiation;
参考文献
Perio, Bertrand; Dozias, Marie-Joelle; Jacquault, Patrick; Hamelin, Jack
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7867 - 7870
反应条件
Montmorillonite clay KSF
T=80°C; 0.166667 h; Irradiation;
参考文献
Perio, Bertrand; Dozias, Marie-Joelle; Jacquault, Patrick; Hamelin, Jack
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7867 - 7870
参考文献
Nozoe, Tetsuo; Wakabayashi, Hidetsugu; Ishikawa, Sumio; Wu, Chi-Phi; Yang, Paw-Wang
Heterocycles, 1990 , vol. 31, # 1 p. 17 - 22
反应条件
copper(I) bromide in benzene
24 h; Heating;
参考文献
Meier, Lothar; Scharf, Hans-Dieter
Synthesis, 1987 , # 5 p. 517 - 520
反应条件
fluorine
Irradiationother time, reagents ratio; Product distribution;
参考文献
Adcock, James L.; Horita, Kiyoshi; Renk, Ehrengard B.
Journal of the American Chemical Society, 1981 , vol. 103, # 23 p. 6937 - 6947