N,N,N',N',N'',N''-hexamethylphosphoric triamide; magnesium bromide; lithium diisopropyl amide in tetrahydrofuran
T=0°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Larcheveque, Marc; Debal, Alain
Journal of the Chemical Society, Chemical Communications, 1981 , # 17 p. 877 - 878
N,N,N',N',N'',N''-hexamethylphosphoric triamide; magnesium bromide; lithium diisopropyl amide in tetrahydrofuran
T=0°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Larcheveque, Marc; Debal, Alain
Journal of the Chemical Society, Chemical Communications, 1981 , # 17 p. 877 - 878
1: (carbomethoxymethyl)trimethylsilane With lithium hexamethyldisilazane in tetrahydrofuran
T=0°C; 0.5 h;
2: cyclohexanone in tetrahydrofuran
T=-78°C; 2 h; Further stages.;
参考文献
Gillies, Malcolm B.; Tonder, Janne E.; Tanner, David; Norrby, Per-Ola
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7378 - 7388
