3,7-二甲基辛-6-烯-1-炔-3-基乙酸酯合成路线 (共 24 条)
参考文献
Saucy et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 1945,1954
参考文献
Saucy et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 1945,1954
参考文献
Saucy et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 1945,1954
反应条件
sulfuric acid; tetraethylammonium bromide in acetonitrile
T=61 - 63°C; by electrolysis; Pt-electrodes;
参考文献
Uneyama, Kenji; Ono, Michio; Torii, Sigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 35 - 44
反应条件
sulfuric acid; tetraethylammonium bromide
Ambient temperatureconstant current, 20 mA, 2.0 F/mol, Pt foils, undivided cell; Yield given. Title compound not separated from byproducts;
参考文献
Torii, Sigeru; Uneyama, Kenji; Ono, Michio
Tetrahedron Letters, 1980 , vol. 21, p. 2741 - 2744
反应条件
tetraethylammonium bromide; magnesium sulfate; diphenyl diselenide in acetonitrile
by electrolysis; Pt-electrodes; different amount of electricity , catalyst and MgSO4; further inorganic salts; different temperatures; Product distribution;
参考文献
Uneyama, Kenji; Ono, Michio; Torii, Sigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 35 - 44
反应条件
diphenyl diselenide; magnesium sulfate
T=66 - 68°C; electrolysis under a constant current 6.7 mA/cm2;
参考文献
Torii, Sigeru; Uneyama, Kenji; Ono, Michio; Bannou, Tadashi
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4606 - 4608
反应条件
tetraethylammonium bromide; magnesium sulfate in acetonitrile
by electrolysis; Pt-electrodes; Mechanism;
参考文献
Uneyama, Kenji; Ono, Michio; Torii, Sigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 35 - 44
反应条件
tetraethylammonium bromide; magnesium sulfate; diphenyl diselenide in acetonitrile
by electrolysis; Pt-electrodes; different amount of electricity , catalyst and MgSO4; further inorganic salts; different temperatures; Product distribution;
参考文献
Uneyama, Kenji; Ono, Michio; Torii, Sigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 35 - 44
反应条件
N(Et)4ClO4; magnesium sulfate; diphenyl diselenide in water; acetonitrile
Ambient temperatureby electrolysis; Pt-electrodes; different H2O/MeOH rates; Product distribution;
参考文献
Uneyama, Kenji; Ono, Michio; Torii, Sigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 35 - 44