反应条件
in further solvent(s) (O2-free) oleic acid and 1-octadecene were added to the mixt. of CF3CO2Na and rare-earth-compound at room temp., heated to 100°C with stirring under vac. for 30 min, heated at 330°C (20K/min) for 30 minunder Ar; excess of ethanol was added at room temp., the mixt. was centrifugally sepd., nanocrystals were washed with ethanol several times, dried in air at 70°C overnight; analysed by X-ray diffraction and transmissionelectron microscopy;
参考文献
Mai, Hao-Xin; Zhang, Ya-Wen; Si, Rui; Yan, Zheng-Guang; Sun, Ling-Dong; You, Li-Ping; Yan, Chun-Hua
Journal of the American Chemical Society, 2006 , vol. 128, # 19 p. 6426 - 6436
