1-硫代-b-D-吡喃葡萄糖苷对甲苯酯合成路线 (共 42 条)
反应条件
DMEG; triethylamine in water; acetonitrile T=-15°C; 1 h; optical yield given as percent de;
参考文献
Tanaka, Tomonari; Matsumoto, Takeshi; Noguchi, Masato; Kobayashi, Atsushi; Shoda, Shin-Ichiro
Chemistry Letters, 2009 , vol. 38, # 5 p. 458 - 459
反应条件
1: hexamethyldisilazane, pyridine 2: zinc iodide, tetrabutylammonium iodide / 1,2-dichloro-ethane / 8 h / 60 °C View Scheme
参考文献
Hanessian, Stephen; Guindon, Yvan
Carbohydrate Research, 1980 , vol. 86, p. C3 - C6
反应条件
1.1: pyridine 1.2: 90 percent / BF3*Et2O 2.1: 100 percent / MeONa / methanol View Scheme
参考文献
Peri, Francesco; Cipolla, Laura; Forni, Eleonora; Nicotra, Francesco
Monatshefte fur Chemie, 2002 , vol. 133, # 4 p. 369 - 382
反应条件
1: 75 percent / CHCl3; ethanol / 0.75 h / Heating 2: 94 percent / 0.4percent sodium methoxide / methanol / 24 h / Ambient temperature View Scheme
参考文献
Wang, Yali; Zhang, Hong; Voelter, Wolfgang
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995 , vol. 50, # 4 p. 661 - 666
反应条件
1: SnCl4 / 1,2-dichloro-ethane / 3 h / Ambient temperature 2: 2 N MeONa / methanol / 20 h View Scheme
参考文献
Kohata, Katsunori; Meguro, Hiroshi
Agricultural and Biological Chemistry, 1982 , vol. 46, # 4 p. 919 - 926
反应条件
sodium methylate in methanol 20 h;
参考文献
Kohata, Katsunori; Meguro, Hiroshi
Agricultural and Biological Chemistry, 1982 , vol. 46, # 4 p. 919 - 926
参考文献
Kohata, Katsunori; Konno, Toshio; Meguro, Hiroshi
Tetrahedron Letters, 1980 , vol. 21, p. 3771 - 3774
反应条件
pyridine; tri-n-butylammonium iodide; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) iodide 2.) 1,2-dichloroethane, 60 deg C, 8 h; Multistep reaction;
参考文献
Hanessian, Stephen; Guindon, Yvan
Carbohydrate Research, 1980 , vol. 86, p. C3 - C6
参考文献
Kohata, Katsunori; Meguro, Hiroshi
Agricultural and Biological Chemistry, 1981 , vol. 45, # 8 p. 1891 - 1894
反应条件
DCN in acetonitrile 72 h; Irradiation; Product distributionMechanism;
参考文献
Griffin, Gary W.; Bandara, Nayanie C.; Clarke, Margaret A.; Tsang, Wing-Sum; Garegg, Per J.; et al.
Heterocycles, 1990 , vol. 30, # 2 p. 939 - 947