1,4-二(苯基氨基)蒽醌合成路线 （共 13 条）
反应条件
in dimethyl sulfoxide
T=80°C; 24 h;
参考文献
Krapcho, A. Paul; Getahun, Zelleka; Avery, Kenneth L.; Vargas, Kevin J.; Hacker, Miles P.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 8 p. 2373 - 2380
反应条件
in dimethyl sulfoxide
T=150°C; 2 h;
参考文献
UNTEGRATED DNA TECHNOLOGIES, INC.
Patent: WO2004/26804 A1, 2004 ;
Location in patent: Page 23-24 ;
反应条件
1: .9 g / H3BO3 / acetic acid / 2 h / 125 °C
2: .3 g / nitrobenzene / 1.5 h / 125 °C
View Scheme
参考文献
Lycka, Antonin; Havlickova, Libuse; Kolonicny, Alois; Jirman, Josef
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 3 p. 736 - 741
反应条件
1: .9 g / H3BO3 / acetic acid / 2 h / 125 °C
2: .3 g / nitrobenzene / 1.5 h / 125 °C
View Scheme
参考文献
Lycka, Antonin; Havlickova, Libuse; Kolonicny, Alois; Jirman, Josef
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 3 p. 736 - 741
反应条件
boric acid; acetic acid
T=120 - 125°C;
参考文献
Grandmougin
Journal fuer Praktische Chemie (Leipzig), 1907 , vol. <2> 76, p. 140
Chem. Zentralbl., 1908 , vol. 79, # I p. 2178
反应条件
air; sodium amide
T=60°C;
参考文献
BASF
Patent: DE360530 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 855
反应条件
1: sulfuric acid monohydrate / 160 °C
2: copper powder; potassium acetate
View Scheme
参考文献
Ullmann; Billig
Justus Liebigs Annalen der Chemie, 1911 , vol. 381, p. 12
反应条件
potassium acetate; copper
参考文献
Ullmann; Billig
Justus Liebigs Annalen der Chemie, 1911 , vol. 381, p. 12
反应条件
unter Durchleiten von Luft;
参考文献
Gen. Aniline Works
Patent: US2051004 , 1934 ;
参考文献
Grandmougin
Journal fuer Praktische Chemie (Leipzig), 1907 , vol. <2> 76, p. 140
Chem. Zentralbl., 1908 , vol. 79, # I p. 2178
