反式-4-氧基-2-丁烯酸乙酯合成路线 (共 44 条)
反应条件
in dichloromethane T=10°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 18, # 16-17 p. 1913 - 1918
反应条件
VS; dihydrogen peroxide T=20°C; 6 h; Further byproducts given;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 34, # 8 p. 900 - 906
反应条件
1: BH3*THF 2: MnO2 View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 47 p. 8515 - 8518
反应条件
acide p-toluenesulfonique; potassium carbonate 1.) cyclohexane, reflux; 2.) water, acetone, reflux, l.5 h; Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 28, # 44 p. 5301 - 5302
反应条件
dimethylsulfide; ozone Solvent Red 19 (Table 2); Yield given. Multistep reaction;
参考文献
Synthesis, , # 10 p. 807 - 810
参考文献
Anales de la Real Sociedad Espanola de Fisica y Quimica, Serie B: Quimica, , vol. 54, p. 689,693
反应条件
hydrogenchloride Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 4353 - 4355
参考文献
Helvetica Chimica Acta, , vol. 32, p. 1017
反应条件
1: With TsNHOH; potassium carbonate in ethanol T=0°C; 2: With triethylamine; p-toluenesulfonyl chloride in acetonitrile T=20°C; 4 h; regioselective reaction;
参考文献
Tang, Shibing; He, Jinmei; Sun, Yongquan; He, Liuer; She, Xuegong
Organic Letters, 2009 , vol. 11, # 17 p. 3982 - 3985
反应条件
1: dichloromethane / 0 °C / |Inert atmosphere 2: triethylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.17 h / 0 °C / |Inert atmosphere 3: 20 °C View Scheme
参考文献
Billedeau, Roland J.; Klein, Klara R.; Kaplan, Daniel; Lou, Yan
Organic Letters, 2013 , vol. 15, # 7 p. 1421 - 1423