反应条件
1.1: sodium acetate / ethanol / 1 h / 20 °C 1.2: 1 h / 20 °C 1.3: 2.5 h / Reflux 2.1: acetic acid; zinc / 20 °C / Cooling with ice 3.1: Candida antarctica lipase type B / acetone / 24 h / 30 °C / pH 7.5 / aq. phosphate buffer 4.1: dimethylsulfide borane complex / tetrahydrofuran / -10 - 67 °C View Scheme
参考文献
Chu, Aurea M.; Fettinger, James C.; David, Sheila S.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 17 p. 4969 - 4972