2-邻甲苯-1H-苯并咪唑合成路线 （共 22 条）
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; 10 palladium on activated carbon in acetic acid
T=120°C; 15 h; Inert atmosphere;
参考文献
Xing, Rui-Guang; Li, Ya-Nan; Liu, Qiang; Meng, Qing-Yuan; Li, Jing; Shen, Xiao-Xia; Liu, Zhengang; Zhou, Bo; Yao, Xiaojun; Liu, Zhong-Li
European Journal of Organic Chemistry, 2010 , # 34 p. 6627 - 6632
反应条件
trifluoromethylsulfonic anhydride; triphenyl-phosphine oxide in 1,2-dichloro-ethane
T=25°C; 0.5 h;
参考文献
Hendrickson, James B.; Hussoin, Md. Sajjat
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4137 - 4139
反应条件
sodium disulfite in N,N-dimethyl-formamide
2 h; Reflux;
参考文献
Khan, Khalid Mohammed; Khan, Momin; Ambreen, Nida; Rahim, Fazal; Naureen, Shagufta; Perveen, Shahnaz; Choudhary, M. Iqbal; Voelterc, Wolfgang
Medicinal Chemistry, 2012 , vol. 8, # 3 p. 421 - 427
反应条件
1: With copper (II) acetate monohydrate; pivalic acid sodium salt in N,N-dimethyl-formamide
T=50°C; Chan-Lam Coupling;
2: With oxygen in N,N-dimethyl-formamide
T=120°C;
参考文献
Li, Jihui; Benard, Sebastien; Neuville, Luc; Zhu, Jieping
Organic Letters, 2012 , vol. 14, # 23 p. 5980 - 5983
反应条件
copper(I) oxide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in water
T=100°C; 30 h; Sealed tube;
参考文献
Peng, Jinsong; Ye, Min; Zong, Cuijuan; Hu, Fangyun; Feng, Lingtong; Wang, Xiaoyan; Wang, Yufeng; Chen, Chunxia
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 716 - 719
反应条件
[Fe(phthalocyanine)]; sodium t-butanolate in toluene
T=120°C; 36 h; Inert atmosphere;
参考文献
Bala, Manju; Verma, Praveen Kumar; Sharma, Upendra; Kumar, Neeraj; Singh, Bikram
Green Chemistry, 2013 , vol. 15, # 6 p. 1687 - 1693
反应条件
copper(ll) bromide in toluene
T=100°C; 24 h;
参考文献
Xiao, Tiebo; Xiong, Shengwei; Xie, Yang; Dong, Xichang; Zhou, Lei
RSC Advances, 2013 , vol. 3, # 36 p. 15592 - 15595
反应条件
copper(I) oxide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in water
T=100°C; 30 h; Sealed tube;
参考文献
Peng, Jinsong; Ye, Min; Zong, Cuijuan; Hu, Fangyun; Feng, Lingtong; Wang, Xiaoyan; Wang, Yufeng; Chen, Chunxia
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 716 - 719
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in water; acetonitrile
T=150°C; Suzuki coupling; 0.5 h; Microwave irradiation;
参考文献
Savall, Brad M.; Fontimayor, Jill R.
Tetrahedron Letters, 2008 , vol. 49, # 47 p. 6667 - 6669
反应条件
sodium hydrogencarbonate; copper(I) bromide in dimethyl sulfoxide
T=120°C; 24 h;
参考文献
Qiu, Dezhi; Wei, Haidong; Zhou, Lihong; Zeng, Qingle
Applied Organometallic Chemistry, 2014 , vol. 28, # 2 p. 109 - 112
