2-溴-5-羟基-4-甲氧基苯甲醛合成路线 （共 39 条）
反应条件
sodium methylate; dimethyl sulfoxide; benzyl alcohol T=150°C; 0.333333 h;
参考文献
Heterocycles, , vol. 31, # 6 p. 1067 - 1076
反应条件
in dimethyl sulfoxide T=150°C; 0.0194444 h;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 4 p. 1287 - 1293
反应条件
sodium methylate; dimethyl sulfoxide T=150°C; 0.133333 h;
参考文献
Heterocycles, , vol. 31, # 6 p. 1067 - 1076
反应条件
1: 79 percent / Br2 / dimethylformamide 2: 66 percent / TMSCl; NaI / CH2Cl2 View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 47, # 10 p. 1512 - 1513
反应条件
1: 40 percent / 2percent NaOH / H2O / 0.83 h / 90 °C 2: 2.2 mg / conc. HCl / ethanol View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 4 p. 1287 - 1293
反应条件
1: potassium bromide; bromine / water / 20 °C 2: hydrogenchloride / water / 10 h / 90 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 6 p. 2583 - 2591
反应条件
bromine; acetic acid
参考文献
Journal of the Chemical Society, , p. 2279,2287
Journal of Organic Chemistry, , vol. 5, p. 204,208
反应条件
sodium methylate; dimethyl sulfoxide T=150°C; 0.0194444 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Imakura, Yasuhiro; Okimoto, Kazuto; Gorohata, Chizuru; Kobayashi, Shigeru; Kihara, Masaru; Yamashita, Shinsuke
Heterocycles, 1990 , vol. 31, # 6 p. 1067 - 1076
反应条件
dimethyl sulfoxide T=150°C; 0.0194444 h; other sodium alkoxide - alcohol (or phenol) systems and sodium alkoxide - alcohol - alcohol (or phenol) systems; various temperatures and reaction times; Product distributionMechanism;
参考文献
Imakura, Yasuhiro; Okimoto, Kazuto; Gorohata, Chizuru; Kobayashi, Shigeru; Kihara, Masaru; Yamashita, Shinsuke
Heterocycles, 1990 , vol. 31, # 6 p. 1067 - 1076
参考文献
Journal of the Chemical Society, , p. 2279,2287
Journal of Organic Chemistry, , vol. 5, p. 204,208
