1: in tetrahydrofuran; 1,2-dichloro-ethane T=20°C; 1 h; 2: With sodium tris(acetoxy)borohydride in tetrahydrofuran; 1,2-dichloro-ethane 3 h; 3: With sodium hydrogencarbonate in tetrahydrofuran; water; 1,2-dichloro-ethane
参考文献
Arienti, Kristen L.; Breitenbucher, J. Guy; Buzard, Daniel J.; Edwards, James P.; Hack, Michael D.; Khatuya, Haripada; Kindrachuk, David E.; Lee, Alice; Venable, Jennifer D.
Patent: US2005/70550 A1, 2005 ;
Location in patent: Page/Page column 34 ;
US 20050070550 A1