3-三甲基甲硅烷基丙炔醛合成路线 （共 23 条）
反应条件
in dichloromethane
T=0 - 20°C;
参考文献
Hachiya, Iwao; Ogura, Kana; Shimizu, Makoto
Organic Letters, 2002 , vol. 4, # 16 p. 2755 - 2757
反应条件
1: 81 percent / p-toluenesulfonic acid / benzene / Heating
2: 1.) BuLi / 1.) THF, -65 deg C, 30 min; 2.) THF, overnight, from -65 deg C to 25 deg C
3: H2SO4 / acetone; H2O / 5 h / Heating
View Scheme
参考文献
Kruithof, Klaas J. H.; Schmitz, Robert F.; Klumpp, Gerhard W.
Tetrahedron, 1983 , vol. 39, # 19 p. 3073 - 3082
反应条件
in tetrahydrofuran; diethyl ether
3 h;
参考文献
Young, David G. J.; Burlison, Joseph A.; Peters, Ulf
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3494 - 3497
