1-(2-甲基-2-丙基)-4-(苯基乙炔基)苯合成路线 （共 14 条）
反应条件
C16H28Cl2NPPd; caesium carbonate in acetonitrile T=80°C; Sonogashira Cross-Coupling; 4 h; Inert atmosphere;
参考文献
Pu, Xiaotao; Li, Hongbo; Colacot, Thomas J.
Journal of Organic Chemistry, 2013 , vol. 78, # 2 p. 568 - 581
反应条件
copper(l) iodide; 8-hydroxy-quinoline; sodium salt of phosphorous acid in ethanol T=80°C; Suzuki coupling; 24 h;
参考文献
Wang, Shihua; Wang, Min; Wang, Lei; Wang, Bo; Li, Pinhua; Yang, Jin
Tetrahedron, 2011 , vol. 67, # 26 p. 4800 - 4806
反应条件
pyridine; CuCl2·2H2O; triethylamine; p-benozquinone in dichloromethane T=20°C; 12 h; Schlenk technique;
参考文献
Shi, Leilei; Jia, Wei; Li, Xun; Jiao, Ning
Tetrahedron Letters, 2013 , vol. 54, # 15 p. 1951 - 1955
反应条件
sodium perchlorate; palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 4-BzO-TEMPO in water; acetonitrile T=20°C; Inert atmosphereElectrochemical reaction;
参考文献
Mitsudo, Koichi; Shiraga, Takuya; Mizukawa, Jun-Ichi; Suga, Seiji; Tanaka, Hideo
Chemical Communications, 2010 , vol. 46, # 48 p. 9256 - 9258
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; 1,4-di(diphenylphosphino)-butane in tetrahydrofuran; dimethyl sulfoxide T=110°C; 2 h;
参考文献
Moon, Jeongju; Jang, Mihee; Lee, Sunwoo
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1403 - 1406
反应条件
bis-triphenylphosphine-palladium(II) chloride; oxygen in 1,4-dioxane T=80°C; Sonogashira type coupling; 18 h;
参考文献
Wang, Xuan; Qin, Weiwei; Kakusawa, Naoki; Yasuike, Shuji; Kurita, Jyoji
Tetrahedron Letters, 2009 , vol. 50, # 46 p. 6293 - 6297
反应条件
3C12H6N2O4(2-)*2Y(3+)*3Pd(2+)*6Cl(1-)*11H2O; 1,8-diazabicyclo[5.4.0]undec-7-ene in water T=90°C; Sonogashira Cross-Coupling; 6 h;
参考文献
Huang, Jinping; Wang, Wei; Li, Hexing
ACS Catalysis, 2013 , vol. 3, # 7 p. 1526 - 1536
反应条件
tert.-butylnitrite; trifuran-2-yl-phosphane; palladium diacetate; acetic acid in dimethyl sulfoxide T=20 - 32°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2011 , vol. 47, # 28 p. 7959 - 7961
反应条件
tert.-butylnitrite; trifuran-2-yl-phosphane; palladium diacetate; acetic acid in dimethyl sulfoxide T=20 - 32°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2011 , vol. 47, # 28 p. 7959 - 7961
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium carbonate in N,N-dimethyl-formamide T=110°C; 24 h; Inert atmosphere;
参考文献
Yan, Hong; Lu, Linhua; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
RSC Advances, 2013 , vol. 3, # 2 p. 377 - 381
