正辛基 α-D-葡萄糖苷合成路线 （共 26 条）
反应条件
sodium methylate in methanol T=20°C; Zemplen reaction; 3 h;
参考文献
Ferlin, Nadege; Grassi, Diego; Ojeda, Carlos; Castro, Mariano J.L.; Grand, Eric; Fernandez Cirelli, Alicia; Kovensky, Jose
Carbohydrate Research, 2008 , vol. 343, # 5 p. 839 - 847
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=100°C; 96 h;
参考文献
Abdel Salam; El Sawady
Egyptian Journal of Chemistry, 2004 , vol. 47, # 2 p. 127 - 142
反应条件
hydrogenchloride T=50°C; 72 h;
参考文献
Kikuchi, Yasuaki; Tanaka, Yasutaka; Sutarto, Supriyanto; Kobayashi, Kenji; Toi, Hiroo; Aoyama, Yasuhiro
Journal of the American Chemical Society, 1992 , vol. 114, # 26 p. 10302 - 10306
反应条件
in methanol; chloroform
参考文献
Hokkaido Electric Power Company, Incorporated; Nishimura, Shin-Ichiro
Patent: US6512109 B1, 2003 ;
反应条件
1: With N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide in dichloromethane T=20°C; 48 h; Molecular sieve; 2: With methanol T=20°C; 3 h; Product distribution / selectivity;
参考文献
WO2008/124729 A1, ;
Page/Page column 16; 25-26 ;
反应条件
palladium on activated charcoal; hydrogen T=20°C; 13 h; Overall yield = 90 percent;
参考文献
Chemistry Letters, , vol. 42, # 10 p. 1235 - 1237
反应条件
sulfuric acid in 1,4-dioxane Yields of byproduct given;
参考文献
Adasch, Volker; Hoffmann, Bettina; Milius, Wolfgang; Platz, Gerhard; Voss, Gundula
Carbohydrate Research, 1998 , vol. 314, # 3-4 p. 177 - 187
反应条件
C2HF6NO4S2*CH2N4 in water T=80°C; 24 h; Reagent/catalyst; Overall yield = 40 percent; stereoselective reaction;
参考文献
Carbohydrate Research, , vol. 381, p. 12 - 18
反应条件
1: BF3*Et2O / CH2Cl2 / 240 h / 20 °C 2: Et3N / methanol; H2O / 24 h / 20 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 1 p. 132 - 134
反应条件
1: BF3*Et2O / CH2Cl2 / 240 h / 20 °C 2: Et3N / methanol; H2O / 24 h / 20 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 1 p. 132 - 134
