正辛基 α-D-葡萄糖苷合成路线 (共 26 条)
反应条件
C9H11N5*C2HF6NO4S2 in water T=80°C; 24 h; Reagent/catalyst; Overall yield = 14 percent; stereoselective reaction;
参考文献
Carbohydrate Research, , vol. 381, p. 12 - 18
反应条件
Amberlyst 15DRY T=110°C; 24 h; Sealed vialIonic liquid;
参考文献
Green Chemistry, , vol. 12, # 10 p. 1790 - 1795
反应条件
Rhizopus sp. amyloglucosidase in di-isopropyl ether; water 72 h; Title compound not separated from byproducts;
参考文献
European Journal of Medicinal Chemistry, , vol. 41, # 9 p. 1059 - 1072
反应条件
1: 2.) acetic anhydride, pyridine / 1.) CH2Cl2, reflux, 6 h, 2.) room temperature, 24 h View Scheme
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
Amberlyst 15DRY T=110°C; 24 h; Sealed vialIonic liquid;
参考文献
Green Chemistry, , vol. 12, # 10 p. 1790 - 1795
反应条件
iron(III) chloride in tetrahydrofuran 24 h; Ambient temperaturevarious solvents and promoters investigated; Product distribution;
参考文献
Tetrahedron Letters, , vol. 36, # 16 p. 2749 - 2752
反应条件
Na2B4O7 in di-isopropyl ether; water pH=8.0; Heating; Kinetics;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 46, # 2 p. 314 - 319
反应条件
oxygen; platinum on activated charcoal in water T=49.9°C; P=300.02 Torr; initial rate of consumption, pH effect; Product distributionMechanism;
参考文献
Vleeming, Johannes H.; Kuster, Ben F.M.; Marin, Guy B.
Carbohydrate Research, 1997 , vol. 303, # 2 p. 175 - 183
反应条件
Sodium bromate; phosphate buffer; Ru(azpy)2(H2O)22+ T=60°C; other pH: 3, 4.5, 8.5, 10; Product distributionMechanism;
参考文献
Boelrijk, Alexandra E. M.; Dorst; Reedijk, Jan
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 11-12 p. 536 - 541
反应条件
Sodium bromate; phosphate buffer; Ru(azpy)2(H2O)22+ T=60°C; other pH: 3, 4.5, 8.5, 10; Product distributionMechanism;
参考文献
Boelrijk, Alexandra E. M.; Dorst; Reedijk, Jan
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 11-12 p. 536 - 541