1,3,5-苯三醇三乙酸酯合成路线 （共 28 条）
反应条件
zinc(II) chloride T=130°C;
参考文献
Chauthe, Siddheshwar K.; Bharate, Sandip B.; Periyasamy, Giridharan; Khanna, Amit; Bhutani, Kamlesh K.; Mishra, Prabhu D.; Singh, Inder P.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 6 p. 2251 - 2256
参考文献
Bazin, Marc-Antoine; Bodero, Lizeth; Tomasoni, Christophe; Rousseau, Benedicte; Roussakis, Christos; Marchand, Pascal
European Journal of Medicinal Chemistry, 2013 , vol. 69, p. 823 - 832
反应条件
1: 1,3,5-tri-iso-propylbenzene With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile
T=75°C; P=22800 Torr; 24 h;
2: With sulfuric acid in acetonitrile
T=20°C; 2 h;
3: acetic anhydride With pyridine
T=120°C; 2 h;
参考文献
Aoki, Yasuhiro; Hirai, Naruhisa; Sakaguchi, Satoshi; Ishii, Yasutaka
Tetrahedron, 2005 , vol. 61, # 46 p. 10995 - 10999
反应条件
1: phloroglucinol trimethyl ether With boron tribromide in dichloromethane
T=0 - 20°C; Inert atmosphere;
2: acetic acid in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Balaydin, Halis T.
Journal of Chemical Research, 2012 , vol. 36, # 4 p. 238 - 240
反应条件
iodine
T=85 - 90°C; 0.75 h;
参考文献
Ahmed, Naseem; van Lier, Johan E.
Tetrahedron Letters, 2006 , vol. 47, # 30 p. 5345 - 5349
反应条件
in pyridine; dichloromethane
0.5 h; from 0 deg C to RT;
参考文献
Menzler, Stefan; Bikker, Jack A.; Horwell, David C.
Tetrahedron Letters, 1998 , vol. 39, # 41 p. 7619 - 7622
反应条件
water; acetic anhydride
参考文献
Heller
Chemische Berichte, 1912 , vol. 45, p. 418
参考文献
Isoshima
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 425,426
Chem.Abstr., 1958 , p. 8948
反应条件
ruthenium(IV) oxide; sodium periodate
1) 5 h, room temp., pyridine; 2) acetone, water, 20 min : decomposition reaction;
参考文献
Mentlein, Rolf; Vowinkel, Erich; Wolf, Bernd
Liebigs Annalen der Chemie, 1984 , # 2 p. 401 - 406
反应条件
ruthenium(IV) oxide; sodium periodate
1) 5 h, room temp., pyridine; 2) acetone, water, 20 min : decomposition reaction;
参考文献
Mentlein, Rolf; Vowinkel, Erich; Wolf, Bernd
Liebigs Annalen der Chemie, 1984 , # 2 p. 401 - 406
