5-苯基-1,3,4-噁二唑-2-硫醇合成路线 (共 46 条)
反应条件
potassium phosphate in water T=20°C; 2.16667 h; Reflux;
参考文献
Yan, Xu; Zhou, Shuo; Wang, Yuanqiang; Ge, Zemei; Cheng, Tieming; Li, Runtao
Tetrahedron, 2012 , vol. 68, # 38 p. 7978 - 7983
反应条件
in dimethyl sulfoxide 0.00833333 h; Irradiation;
参考文献
Joshi, Sachin; Karnik
Synthetic Communications, 2002 , vol. 32, # 1 p. 111 - 114
反应条件
hydrazine hydrate in ethanol 4 h; Heating;
参考文献
Sasaki, Tadashi; Ito, Eikoh; Shimizu, Ikuo
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2757 - 2760
反应条件
1: 94 percent / hydrazine hydrate / ethanol 2: 90 percent / dimethylformamide View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 16 p. 4842 - 4850
反应条件
1: Acidic conditions 2: hydrazine hydrate 3: potassium hydroxide View Scheme
参考文献
Molecules, , vol. 16, # 2 p. 1297 - 1309
反应条件
in N,N-dimethyl-formamide
参考文献
Macaev, Fliur; Rusu, Ghenadie; Pogrebnoi, Serghei; Gudima, Alexandru; Stingaci, Eugenia; Vlad, Ludmila; Shvets, Nathaly; Kandemirli, Fatma; Dimoglo, Anatholy; Reynolds, Robert
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 16 p. 4842 - 4850
反应条件
in N,N-dimethyl-formamide 0.0833333 h; Microwave irradiation; TemperatureTime;
参考文献
Mahesh Kumar; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 11 p. 1619 - 1622
反应条件
1: hydrazine hydrate / methanol / 6 h / Heating 2: KOH / ethanol / 8 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 8 p. 2278 - 2282
反应条件
1: triethylamine / CH2Cl2 2: Na2CO3 / dimethylsulfoxide; H2O 3: 80 percent / Ambient temperature; other substrate View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 57, # 1/2 p. 11 - 15
反应条件
1: triethylamine / dichloromethane / 0 °C 2: hydrazine hydrate / methanol / 5 h / |Reflux 3: potassium hydroxide / methanol / 20 °C / |Reflux 4: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194