in tetrahydrofuran other Radiation; microwave-accelerated preparation of arylzinc iodide by Rieke zinc insertion into aryl iodide under sealed vessel conditions for 10 min; THF 180°C; HPLC or MS;

1: 2-chloro-5-carboxybenzene With Merriefield resin; caesium carbonate in 1-methyl-pyrrolidin-2-one T=200°C; 0.0833333 h; microwave irradiation; 2: (3-methoxyphenyl)zinc(II) iodide With tris(dibenzylideneacetone)dipalladium (0); tBuP*HBF4 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=175°C; Negishi cross-coupling; 0.166667 h; microwave irradiation; 3: With trifluoroacetic acid in dichloromethane T=160°C; 0.0833333 h; microwave irradiation;