sodium hydroxide; dihydrogen peroxide; dichloro(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) in tetrahydrofuran; hexane To a soln. of 9-octyl-9-BBN is added a soln. of BuLi at -60°C, react. mixt. warmed up to room temp. for 30 min, iodobenzene and catalyst are added, mixt. refluxed for 5 h, oxidized by addn. of aq. NaOH and H2O2 at room temp. for 1h.; Identified by GLC and mass spectrometry.;
参考文献
Journal of the American Chemical Society, , vol. 111, # 1 p. 314 - 321
