2-二乙基膦酰基-2-氟乙酸合成路线 （共 17 条）
反应条件
sodium hydroxide in water T=20°C; 20 h;
参考文献
Sano, Shigeki; Teranishi, Rie; Nagao, Yoshimitsu
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9183 - 9186
反应条件
hydrogenchloride; n-butyllithium; chloro-trimethyl-silane 1.) THF, hexane, -78 deg C, 10 min, 2.) -60 deg C, 15 min; 20 deg C, 10 min, 3.) CH2Cl2, 10 min; Yield given. Multistep reaction;
参考文献
Waschbuesch, Rachel; Carran, John; Savignac, Philippe
Tetrahedron, 1997 , vol. 53, # 18 p. 6391 - 6400
反应条件
n-butyllithium in tetrahydrofuran T=0°C; Horner-Wadsworth-Emmons reaction; 12 h;
参考文献
Sano, Shigeki; Teranishi, Rie; Nagao, Yoshimitsu
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9183 - 9186
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 1 h; 2.) 15 h room temperature;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 1 h; 2.) 15 h room temperature;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 3 h; 2.) 15 h room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 3 h; 2.) 15 h room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 3 h; 2.) 15 h room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 3 h; 2.) 15 h room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 3 h; 2.) 15 h room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
