4-(羟甲基)苯硼酸频哪醇酯合成路线 （共 16 条）
反应条件
sodium sulfate in tetrahydrofuran 2 h; Inert atmosphere;
参考文献
Broaders, Kyle E.; Grandhe, Sirisha; Frechet, Jean M. J.
Journal of the American Chemical Society, 2011 , vol. 133, # 4 p. 756 - 758
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in dimethyl sulfoxide T=85°C; 18 h; Inert atmosphere;
参考文献
EP2450354 A1, ;
Page/Page column 19-20 ;
反应条件
potassium acetate; bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane T=80°C; 24 h; Inert atmosphere;
参考文献
US2012/184520 A1, ;
Page/Page column 17 ;
反应条件
sodium tetrahydroborate in methanol T=4°C; 0.166667 h;
参考文献
De Filippis, Arnault; Morin, Christophe; Thimon, Christian
Synthetic Communications, 2002 , vol. 32, # 17 p. 2669 - 2676
反应条件
AlCl3, aluminium chloride in ethanol T=20°C;
参考文献
Quin, Caroline; Robertson, Linsey; McQuaker, Stephen J.; Price, Nicholas C.; Brand, Martin D.; Hartley, Richard C.
Tetrahedron, 2010 , vol. 66, # 13 p. 2384 - 2389
反应条件
1: 100 percent / tetrahydrofuran; toluene 2: 80 percent / NaBH4 / methanol / 0.17 h / 4 °C View Scheme
参考文献
Synthetic Communications, , vol. 32, # 17 p. 2669 - 2676
反应条件
1: magnesium sulfate / methanol / 6 h / 20 °C 2: sodium tetrahydroborate / 5 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
