1-(5-乙酰基萘-1-基)乙酮合成路线 (共 4 条)
反应条件
carbon disulfide; aluminium trichloride T=60°C;
参考文献
Canonne,P.; St-Jean,R.
Bulletin de la Societe Chimique de France, 1971 , p. 3052 - 3057
Full Text Show Details
Buu-Hoi,N.P. et al.
Journal of Heterocyclic Chemistry, 1968 , vol. 5, p. 259 - 262
反应条件
1: 51 percent / PCl5 / CH2Cl2 / 4.5 h / Heating 2: 1100 °C / 0.01 Torr View Scheme
参考文献
Sarobe, Martin; Flink, Simon; Jenneskens, Leonardus W.; Zwikker, Jan W.; Wesseling, Jolanda
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 10 p. 2125 - 2132
反应条件
1: in diethyl ether; toluene 24 h; Heating / reflux; 2: With hydrogenchloride in water T=0°C;
参考文献
Elf Atochem S.A.
Patent: US6660191 B1, 2003 ;
Location in patent: Page column 8 ;
反应条件
bromine; acetic acid
参考文献
Voss, Jurgen; Sarafidis, Abraam; Sawluk, Andrzej; Schmidt, Gunther; Adiwidjaja, Gunadi
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 11 p. 2249 - 2276