T=100°C; nachfolgend Behandlung mit Wasserdampf;

1: AlCl3; CS2 2: zinc; aqueous acetic acid; ethanol View Scheme

暂无反应条件数据

1.1: methanesulfonic acid; phosphorous pentoxide / 4 h / 40 °C 2.1: methanol; potassium acetate / 0.25 h / Reflux 3.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 12 h / 20 °C 4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere 4.2: -78 - 20 °C / Inert atmosphere 5.1: quinoline; hydrogen / hexane; toluene / 1 h / 20 °C / 760.05 Torr 5.2: 0.25 h / 20 °C View Scheme

1: polyphosphoric acid 2: sodium acetate; methanol View Scheme

methanesulfonic acid; phosphorous pentoxide T=40°C; 4 h;