1,2,3,4-四甲基萘合成路线 （共 49 条）
反应条件
n-butyllithium; tungsten hexachloride in tetrahydrofuran; hexane 1.) -78 deg C, 1 h, 2.) from -78 deg C to room temp., 1 h, 3.) 5 h;
参考文献
Hart, Harold; Nwokogu, Godson
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1251 - 1255
反应条件
1: glacial acetic acid; HCl 2: palladium; acetone / Hydrogenolyse 3: glacial acetic acid; HCl 4: palladium; acetone / Hydrogenolyse View Scheme
参考文献
Sasse,W.H.F. et al.
Australian Journal of Chemistry, 1971 , vol. 24, p. 2151 - 2171
反应条件
in benzene T=350°C; 2 h;
参考文献
Sekiguchi, Akira; Zigler, Steven S.; Haller, Kenneth J.; West, Robert
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 197 - 202
反应条件
in benzene T=350°C; 2 h;
参考文献
Sekiguchi, Akira; Zigler, Steven S.; Haller, Kenneth J.; West, Robert
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 197 - 202
反应条件
sodium hydroxide in ethanol; water Heating;
参考文献
Listvan, V. N.; Stasyuk, A. P.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 2 p. 354 - 359
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 2 p. 392 - 398
反应条件
in benzene T=350°C; 2 h;
参考文献
Sekiguchi, Akira; Zigler, Steven S.; Haller, Kenneth J.; West, Robert
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 197 - 202
反应条件
in benzene T=350°C; 2 h; vacuum;
参考文献
Sekiguchi, Akira; Zigler, Steven S.; Haller, Kenneth J.; West, Robert
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 197 - 202
反应条件
hydrogen; sodium acetate; palladium on activated charcoal in acetic acid
参考文献
Sasse,W.H.F. et al.
Australian Journal of Chemistry, 1971 , vol. 24, p. 2151 - 2171
反应条件
1: palladium; acetone / Hydrogenolyse 2: glacial acetic acid; HCl 3: palladium; acetone / Hydrogenolyse View Scheme
参考文献
Hart,H.; Murray,R.K.
Journal of Organic Chemistry, 1967 , vol. 32, p. 2448 - 2452
反应条件
palladium on activated charcoal
参考文献
Kloetzel et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 273,275
