4-甲氧苯基2,4,6-三-O-乙酰-3-O-苄基-β-D-吡喃葡萄糖苷合成路线 (共 4 条)
反应条件
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve in dichloromethane T=0°C; Etherification; Deacetylation; 2 h;
参考文献
Karst, Nathalie; Jacquinet, Jean-Claude
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2709 - 2717
反应条件
in methanol T=20°C; Deacetylation; 16 h;
参考文献
Karst, Nathalie; Jacquinet, Jean-Claude
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2709 - 2717
反应条件
sodium methylate in methanol 3 h;
参考文献
Palmacci, Emma R.; Seeberger, Peter H.
Tetrahedron, 2004 , vol. 60, # 35 p. 7755 - 7766
反应条件
1: NaOMe / methanol / 3 h 2: 810 mg / p-toluenesulfonic acid / acetonitrile / 15 h View Scheme
参考文献
Karst, Nathalie; Jacquinet, Jean-Claude
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2709 - 2717