(2E,4E)-2,4-癸二烯酸合成路线 (共 46 条)
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide T=25°C; 3 h;
参考文献
Abarbri, Mohamed; Parrain, Jean-Luc; Cintrat, Jean-Christophe; Duchene, Alain
Synthesis, 1996 , # 1 p. 82 - 86
反应条件
sodium hydroxide; silver nitrate in ethanol T=20°C;
参考文献
Romano, Giovanna; Miralto, Antonio; Ianora, Adrianna
Marine Drugs, 2010 , vol. 8, # 4 p. 950 - 967
反应条件
potassium hydroxide in methanol 10 h; Ambient temperature;
参考文献
Bari; Sattar; Vig; Kumar; Vasisht
Journal of the Indian Chemical Society, 1990 , vol. 67, # 12 p. 995 - 996
反应条件
n-butyllithium in tetrahydrofuran; benzene T=20°C; 1.5 h;
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 11 p. 2285 - 2286
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 11 p. 2589 - 2590
反应条件
potassium tert-butylate in dimethyl sulfoxide T=25 - 30°C; 1 h;
参考文献
Nakai, Takeshi; Mikami, Koichi; Taya, Shiro; Kimura, Yasuhiro; Mimura, Tetsuya
Tetrahedron Letters, 1981 , vol. 22, p. 69 - 72
反应条件
hydrogenchloride; lithium hydroxide in water; acetone 1.5 h; Heating;
参考文献
Strunz, George M.; Finlay, Heather J.
Canadian Journal of Chemistry, 1996 , vol. 74, # 3 p. 419 - 432
反应条件
1: 81 percent / pyridinium chlorochromate / CH2Cl2 / 1.5 h 2: 83 percent / n-BuLi / tetrahydrofuran; benzene / 1.5 h / 20 °C View Scheme
参考文献
Jacobson
Journal of the American Chemical Society, 1953 , vol. 75, p. 2584 Anm. 11
反应条件
1: 1) n-BuLi / 1) THF, -30 deg C, 1 h, 2) -78 deg C, 5 min 2: p-toluenesulfonic acid / benzene / 4 h / Heating 3: t-BuOK / 2-methyl-propan-2-ol / 12 h / Ambient temperature View Scheme
参考文献
Mandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, Junzo
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 603 - 606
反应条件
1: pyridine; piperidine 2: lithium alanate; diethyl ether 3: potassium dichromate; aqueous sulfuric acid 4: pyridine / Erhitzen des Reaktionsgemisches View Scheme
参考文献
Burden,R.S.; Crombie,L.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2477 - 2481
参考文献
Ono, Noboru; Miyake, Hideyoshi; Tanabe, Yo; Tanaka, Kazuhiko; Kaji, Aritsune
Chemistry Letters, 1980 , p. 1365 - 1368