2,4,6-三乙基环硼氧烷合成路线 （共 34 条）
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2, page 180 - 189
反应条件
1: neat (no solvent) 2: neat (no solvent) View Scheme
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2.2, page 189 - 196
反应条件
in neat (no solvent) Ar; 180°C; vacuum;;
参考文献
Koester, Roland; Sporzynski, Andrzej; Schuessler, Wilhelm; Blaeser, Dieter; Boese, Roland
Chemische Berichte, 1994 , vol. 127, # 7 p. 1191 - 1200
反应条件
in not given under Ar, room temp.; detn. by (17)O-NMR;
参考文献
Koester, Roland; Schuessler, Wilhelm; Blaeser, Dieter; Boese, Roland
Chemische Berichte, 1994 , vol. 127, # 9 p. 1593 - 1598
反应条件
in neat (no solvent) (argon); 120°C, 25 min; NMR monitoring;
参考文献
Koester, Roland; Schuessler, Wilhelm; Boese, Roland; Herberhold, Max; Gerstmann, Silke; Wrackmeyer, Bernd
Chemische Berichte, 1996 , vol. 129, # 5 p. 503 - 507
反应条件
in hexane Ar atmosphere, stirring (20°C, 24 h); not isolated, detd. by (11)B-NMR;
参考文献
Koester, Roland; Seidel, Guenter; Boese, Roland; Wrackmeyer, Bernd
Chemische Berichte, 1988 , vol. 121, p. 597 - 616
参考文献
Gmelin Handbook: B: B-Verb.13, 4.5.3.3, page 160 - 167
Full Text Show Details
McElroy, A. D.; Hunt, R. M.
Patent: US2996539 , 1962 ;
反应条件
in toluene heating at 120°C for 30 min under exclusion of air and moisture; monitored by NMR;
参考文献
Koester, Roland; Tsay, Yi-Hung; Synoradzki, Ludwik
Chemische Berichte, 1987 , vol. 120, p. 1117 - 1124
反应条件
in neat (no solvent) byproducts: Et2Se, ethane, ethene; (argon); 45-65°C (upon heating to 80-85°C, the title compd. disappears and Et2Se2 is formed additionally); removal of volatiles (vac.), recrystn. (heptane); elem. anal.;
参考文献
Koester, Roland; Schuessler, Wilhelm; Boese, Roland; Herberhold, Max; Gerstmann, Silke; Wrackmeyer, Bernd
Chemische Berichte, 1996 , vol. 129, # 5 p. 503 - 507
反应条件
in neat (no solvent) byproducts: Et2Se, Et2Se2; (argon); 55°C, 1 h; NMR monitoring;
参考文献
Koester, Roland; Schuessler, Wilhelm; Boese, Roland; Herberhold, Max; Gerstmann, Silke; Wrackmeyer, Bernd
Chemische Berichte, 1996 , vol. 129, # 5 p. 503 - 507
