3a,4,7,7a-四羟基茚合成路线 （共 33 条）
反应条件
dihydrogen peroxide; acetic acid
参考文献
Alimardanov, Kh. M.; Sadygov; Garibov; Abdullaeva, M. Ya.
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 10 p. 1302 - 1308
Zhurnal Organicheskoi Khimii, 2012 , vol. 48, # 10 p. 1307 - 1312,6
反应条件
boron trifluoride; acetic acid in octane T=112°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 6 p. 1114 - 1124
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1226 - 1237
反应条件
boron trifluoride in hexane T=80°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 6 p. 1114 - 1124
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1226 - 1237
反应条件
boron trifluoride in hexane T=80°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 6 p. 1114 - 1124
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1226 - 1237
反应条件
boron trifluoride in hexane T=80°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 6 p. 1114 - 1124
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1226 - 1237
反应条件
boron trifluoride in hexane T=80°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 6 p. 1114 - 1124
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1226 - 1237
反应条件
boron trifluoride in hexane T=80°C; 1 h; other concentration, other time, other reagent, other solvents, other temperature; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 6 p. 1114 - 1124
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1226 - 1237
反应条件
N-bromosuccinmide; lithium aluminium tetrahydride; sodium iodide 1.15 min, room temp., DMSO aq. 2. 3 h, reflux, THF; Product distribution;
参考文献
Gevorkyan, G. G.; Belikova, N. A.; Bobyleva, A. A.; Pekhk, T. I.; Anfilogova, S. N.; et al.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1583 - 1588
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1732 - 1738
反应条件
hydrogen; palladium on activated charcoal in methanol; pentane
参考文献
Kaufmann, Dieter; Fick, Hans-Heinrich; Schallner, Otto; Spielmann, Werner; Meyer, Lueder-Ulrich; et al.
Chemische Berichte, 1983 , vol. 116, # 2 p. 587 - 609
反应条件
T=160 - 180°C; Cope Rearrangement; P=1147.92 - 2311.54 Torr; 17 - 40 h; PyrolysisIndustry scale; Rate constant;
参考文献
PROMERUS LLC
Patent: US2009/54714 A1, 2009 ;
Location in patent: Page/Page column 10-11 ;
