苯并[b]芘-6,12-二酮合成路线 (共 20 条)
反应条件
1: With iodine; silver perchlorate in benzene Radical cation*AgI formation; 2: With water in acetonitrile Substitution; Title compound not separated from byproducts;
参考文献
Stack; Cremonesi; Hanson; Rogan; Cavalieri
Xenobiotica, 1995 , vol. 25, # 7 p. 755 - 760
反应条件
1: benzo(a)pyrene With iodine; silver perchlorate in benzene Radical cation*AgI formation; 2: sodium acetate in water; acetonitrile Substitution;
参考文献
Stack; Cremonesi; Hanson; Rogan; Cavalieri
Xenobiotica, 1995 , vol. 25, # 7 p. 755 - 760
反应条件
in acetonitrile 1 h; Further byproducts given. Yields of byproduct given;
参考文献
Stack; Cremonesi; Hanson; Rogan; Cavalieri
Xenobiotica, 1995 , vol. 25, # 7 p. 755 - 760
反应条件
1: 6-fluorobenzolt;agt;pyrene With iodine; silver perchlorate in benzene Radical cation*AgI formation; 2: sodium acetate in water; acetonitrile Substitution;
参考文献
Stack; Cremonesi; Hanson; Rogan; Cavalieri
Xenobiotica, 1995 , vol. 25, # 7 p. 755 - 760
反应条件
1: 6-Chlorobenzo[a]pyrene With iodine; silver perchlorate in benzene Radical cation*AgI formation; 2: sodium acetate in water; acetonitrile Substitution;
参考文献
Stack; Cremonesi; Hanson; Rogan; Cavalieri
Xenobiotica, 1995 , vol. 25, # 7 p. 755 - 760
反应条件
oxygen in chloroform 48 h; Irradiationtetraphenylporphyrin as photosensitizer;
参考文献
Lee-Ruff, E.; Kazarians-Moghaddam, H.; Katz, M.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 1297 - 1303
反应条件
in water; acetonitrile 0.25 h; Further byproducts given. Yields of byproduct given;
参考文献
Cremonesi, Paolo; Stack, Douglas E.; Rogan, Eleanor G.; Cavalieri, Ercole L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7683 - 7687
反应条件
<(Ξ)-phthalidyliden>-acetic acid;
参考文献
Schroeder et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 446,449
反应条件
1 h; Irradiation; Product distribution; Further Variations:time;
参考文献
Fukuhara; Kurihara; Miyata
Journal of the American Chemical Society, 2001 , vol. 123, # 36 p. 8662 - 8666
反应条件
sodium hydroxide; zinc
参考文献
Alpert, Andrew J.; Cavalieri, Ercole L.
Journal of Medicinal Chemistry, 1980 , vol. 23, # 8 p. 919 - 927