(三甲基硅基)甲基化异腈合成路线 （共 10 条）
反应条件
in various solvent(s)
参考文献
Livinghouse, Tom; Smith, Richard
Journal of the Chemical Society, Chemical Communications, 1983 , # 5 p. 210 - 211
反应条件
(i) nBuLi, hexane, THF, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Smith, Richard; Livinghouse, Tom
Synthetic Communications, 1984 , vol. 14, # 7 p. 639 - 646
参考文献
Dolby, Lloyd J.; Esfandiari, Shervin; Garst, Michael E.
Patent: US2005/101785 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
2,2'-azo-bisisobutyronitrile; (S-i-pr)3SiH in toluene T=75 - 90°C; Yield given;
参考文献
Chatgilialoglu, C.; Guerra, M.; Guerrini, A.; Seconi, G.; Clark, K. B.; et al.
Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2427 - 2433
参考文献
Dolby, Lloyd J.; Esfandiari, Shervin; Garst, Michael E.
Patent: US2005/101785 A1, 2005 ;
Location in patent: Page/Page column 6 ;
参考文献
Dolby, Lloyd J.; Esfandiari, Shervin; Garst, Michael E.
Patent: US2005/101785 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
copper acetylacetonate
T=50°C; 3 h;
参考文献
Smith, Richard; Livinghouse, Tom
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1554 - 1555
Title/Abstract Full Text View citing articles Show Details
Smith, Richard; Livinghouse, Tom
Tetrahedron, 1985 , vol. 41, # 17 p. 3559 - 3568
反应条件
Cu2Cl2
T=110°C; 2 h;
参考文献
Smith, Richard; Livinghouse, Tom
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1554 - 1555
参考文献
Dolby, Lloyd J.; Esfandiari, Shervin; Garst, Michael E.
Patent: US2005/101785 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
potassium tert-butylate in tetrahydrofuran
T=-15°C; 2.5 h;
参考文献
Dolby, Lloyd J.; Esfandiari, Shervin; Garst, Michael E.
Patent: US2005/101785 A1, 2005 ;
Location in patent: Page/Page column 6 ;
