2-(二甲基氨基)环己烷-1-醇合成路线 （共 9 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Oliveira, Paulo R.; Wiectzycosky, Franciele; Basso, Ernani A.; Goncalves, Regina A.C.; Pontes, Rodrigo M.
Journal of Molecular Structure, 2003 , vol. 657, # 1-3 p. 191 - 198
参考文献
FMC Corporation
Patent: US4040813 A1, 1977 ;
参考文献
Liu, Sheng; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2007 , vol. 46, # 39 p. 7506 - 7508
反应条件
1: 53 percent / H2O / 135 °C 2: 77 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Bocca, Cleverson C.; Rittner, Roberto; Hoeehr, Nelci F.; Pinheiro, Glaucia M.S.; Abiko, Layara A.; Basso, Ernani A.
Journal of Molecular Structure, 2010 , vol. 983, # 1-3 p. 194 - 199
反应条件
1: bromine / 0 - 5 °C 2: water / 135 °C / Autoclave 3: lithium aluminium tetrahydride / tetrahydrofuran View Scheme
参考文献
Bocca, Cleverson C.; Rittner, Roberto; Hoeehr, Nelci F.; Pinheiro, Glaucia M.S.; Abiko, Layara A.; Basso, Ernani A.
Journal of Molecular Structure, 2010 , vol. 983, # 1-3 p. 194 - 199
反应条件
1: (i) aq. H2O2, MeOH, (ii) (pyrolysis) 2: (i) Zn-Cu, Et2O, (ii) /BRN= 2038531/ View Scheme
参考文献
Tsuji,T. et al.
Bulletin of the Chemical Society of Japan, 1967 , vol. 40, # 10 p. 2338 - 2343
反应条件
oxalyl dichloride; triethylamine in dichloromethane; dimethyl sulfoxide
T=20°C; Swern oxidation; 2.5 h;
参考文献
Liu, Sheng; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2007 , vol. 46, # 39 p. 7506 - 7508
反应条件
(i) aq. H2O2, MeOH, (ii) (pyrolysis); Multistep reaction;
参考文献
Tsuji,T. et al.
Bulletin of the Chemical Society of Japan, 1967 , vol. 40, # 10 p. 2338 - 2343
反应条件
in N-methyl-acetamide; para-xylene; water
参考文献
FMC Corporation
Patent: US4040813 A1, 1977 ;
