2,4,6-三甲基-1,3-苯二胺合成路线 (共 12 条)
反应条件
hydrogenchloride; zinc
参考文献
Bl.Soc.franc.Phot., vol. <3> 15, p. 92
Chem. Zentralbl., , vol. 99, # II p. 1415
参考文献
Justus Liebigs Annalen der Chemie, , vol. 179, p. 168
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane 18 h; Yield given;
参考文献
Dvolaitzky, Maya; Chiarelli, Robert; Rassat, Andre
Angewandte Chemie, 1992 , vol. 104, # 2 p. 220 - 222
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Wu, Chengde; Anderson, C. Eric; Bui, Huong; Gao, Daxin; Kassir, Jamal; Li, Wen; Wang, Junmei; Biediger, Ronald; Chen, Jie; Market, Robert V.
Patent: US2005/49286 A1, 2005 ;
US 20050049286 A1
反应条件
tributylphosphine; di-isopropyl azodicarboxylate in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Saylik, Dilek; Horvath, Michael J.; Elmes, Patricia S.; Jackson, W. Roy; Lovel, Craig G.; Moody, Keith
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3940 - 3946
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 0.166667 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias; Schlechtingen, Georg
Angewandte Chemie, 1995 , vol. 107, # 22 p. 2746 - 2749
反应条件
1: pyridine
2: aqueous KOH-solution
View Scheme
参考文献
Adams; Chase
Journal of the American Chemical Society, 1948 , vol. 70, p. 4202
参考文献
Adams; Chase
Journal of the American Chemical Society, 1948 , vol. 70, p. 4202
参考文献
Ladenburg
Justus Liebigs Annalen der Chemie, 1875 , vol. 179, p. 168
反应条件
nach Schotten-Baumann;
参考文献
Adams; Tjepkema
Journal of the American Chemical Society, 1948 , vol. 70, p. 4204,4206,4207