反应条件
in dichloromethane
under N2, CH2Cl2 soln. of (Cp(CO)2FeCH2)PF6 at -78°C treated with Cp(CO)2FeCOMe, kept for 25 min at low temp., warmed to 20°C, (i), ether-insol. solid treated with excess n-Bu4NI, (ii); (i) solid filtered, washed with CH2Cl2, extd. with MeNO2, evapd. (25 mm, 20°C), crystals vac. dried (1E-2 mm, 1 h), filtrate evapd., extd. with degassed Et2O, filtered, evapd.; (ii) IR identification;
参考文献
Bodnar, T. W.; Cutler, A. R.
Organometallics, 1985 , vol. 4, p. 1558 - 1565
