6,7,13,14-四氧杂二螺[4.2.4.2]十四烷合成路线 (共 11 条)
反应条件
dihydrogen peroxide in water
参考文献
Berkessel, Albrecht; Andreae, Marc R. M.; Schmickler, Hans; Lex, Johann
Angewandte Chemie - International Edition, 2002 , vol. 41, # 23 p. 4481 - 4484
反应条件
ozone in pentane T=0°C;
参考文献
Griesbaum, Karl; Krieger-Beck, Petra; Beck, Johannes
Chemische Berichte, 1991 , vol. 124, # 2 p. 391 - 396
反应条件
tetrafluoroboric acid; dihydrogen peroxide; methyltrioxorhenium (VII) in diethyl ether; 2,2,2-trifluoroethanol; water T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Zmitek, Katja; Stavber, Stojan; Zupan, Marko; Bonnet-Delpon, Daniele; Charneau, Sebastien; Grellier, Phillipe; Iskra, Jernej
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 23 p. 7790 - 7795
反应条件
dihydrogen peroxide in hexafluoroisopropyl alcohol; water T=50°C; Baeyer-Villiger oxidation; 1.5 h;
参考文献
Piscopo, Calogero G.; Loebbecke, Stefan; Maggi, Raimondo; Sartori, Giovanni
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1625 - 1629
反应条件
dichloromethane; ozone T=-80°C;
参考文献
Criegee et al.
Justus Liebigs Annalen der Chemie, 1953 , vol. 583, p. 1,28
反应条件
ozone in pentane T=0°C;
参考文献
Griesbaum, Karl; Krieger-Beck, Petra; Beck, Johannes
Chemische Berichte, 1991 , vol. 124, # 2 p. 391 - 396
反应条件
zirconium carboxyethylphosphonate; water; dihydrogen peroxide T=45°C; Baeyer-Villiger oxidation; 24 h;
参考文献
Rocha, Graca M. S. R. O.; Santos, Teresa M.; Bispo, Claudia S. S.
Catalysis Letters, 2011 , vol. 141, # 1 p. 100 - 110
反应条件
sulfuric acid; dihydrogen peroxide; acetic anhydride
参考文献
Dilthey; Huchtemann
Journal fuer Praktische Chemie (Leipzig), 1940 , vol. <2> 154, p. 238,254
参考文献
Gmelin Handbook: S: MVol.B2, 5, page 798 - 808
参考文献
Dilthey; Huchtemann
Journal fuer Praktische Chemie (Leipzig), 1940 , vol. <2> 154, p. 238,254