1,3-二碘-2-甲氧基-5-硝基苯合成路线 (共 9 条)
反应条件
potassium carbonate in acetone T=65°C; 18 h; Inert atmosphere;
参考文献
Beale, Thomas M.; Allwood, Daniel M.; Bender, Andreas; Bond, Peter J.; Brenton, James D.; Charnock-Jones, D. Stephen; Ley, Steven V.; Myers, Rebecca M.; Shearman, James W.; Temple, Jill; Unger, Jessica; Watts, Ciorsdaidh A.; Xian, Jian
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 3 p. 177 - 181
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C; 60 h;
参考文献
Helgeson, Roger C.; Czech, Bronislaw P.; Chapoteau, Eddy; Gebauer, Carl R.; Kumar, Anand; Cram, Donald J.
Journal of the American Chemical Society, 1989 , vol. 111, # 16 p. 6339 - 6350
反应条件
sodium periodate; sulfuric acid; potassium iodide T=25 - 30°C; 2 h;
参考文献
Kraszkiewicz, Lukasz; Sosnowski, Maciej; Skulski, Lech
Synthesis, 2006 , # 7 p. 1195 - 1199
反应条件
potassium carbonate; nitrobenzene T=130°C;
参考文献
Journal of the American Chemical Society, , vol. 64, p. 1070,1072
反应条件
1: hydrogenchloride; sodium chlorite; sodium iodide / methanol; water / 18 h / 0 - 20 °C 2: potassium carbonate / acetone / 18 h / 65 °C / Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 5 p. 1749 - 1759
反应条件
nitric acid; acetic acid T=65°C;
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 27, p. 402
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 27, p. 402
反应条件
1: durch Methylierung 2: glacial acetic acid; fuming nitric acid / 65 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 27, p. 402
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 27, p. 402