二氢-3-碘呋喃-2(3H)-酮合成路线 (共 5 条)
反应条件
sodium iodide in acetone T=20°C; 8 h;
参考文献
Denmark, Scott E.; Yang, Shyh-Ming
Journal of the American Chemical Society, 2004 , vol. 126, # 39 p. 12432 - 12440
反应条件
dihydrogen peroxide; iodine in diethyl ether T=0°C; 0.5 h; Overall yield = 0.42 g;
参考文献
Terent'Ev, Alexander O.; Zdvizhkov, Alexander T.; Kulakova, Alena N.; Novikov, Roman A.; Arzumanyan, Ashot V.; Nikishin, Gennady I.
RSC Advances, 2014 , vol. 4, # 15 p. 7579 - 7587
反应条件
iodonium di-sym-collidine tetrafluoroborate; dimethyl sulfoxide in dichloromethane 2 h; Ambient temperature;
参考文献
Evans, Robert D.; Schauble, J. Herman
Synthesis, 1986 , # 9 p. 727 - 730
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=30°C; 20 h;
参考文献
Simpson, James H.; Stille, J. K.
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1759 - 1760
反应条件
manganese in tetrahydrofuran
T=25°C; 2.5 h;
参考文献
Kakiya, Hirotada; Nishimae, Shinji; Shinokubo, Hiroshi; Oshima, Koichiro
Tetrahedron, 2001 , vol. 57, # 42 p. 8807 - 8815