2-氯-4,6-二甲氧基-1,3,5-三嗪合成路线 (共 40 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether
68 h; Heating;
参考文献
Samaritani, Simona; Signore, Giovanni; Malanga, Corrado; Menicagli, Rita
Tetrahedron, 2005 , vol. 61, # 18 p. 4475 - 4483
反应条件
in benzene
T=10°C; 12 h;
参考文献
Chesniuk; Mikhailichenko; Zavodnov; Zaplishny
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 2 p. 177 - 182
反应条件
trimethylamine in tetrahydrofuran; acetone
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4496392 A1, 1985 ;
反应条件
4-methyl-morpholine in dichloromethane
1.) 0 to 5 deg C, 5 h 2.) r.t., 10 h;
参考文献
Kaminski, Zbigniew J.
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 4 p. 579 - 583
参考文献
Am.Cyanamid Co.
Patent: US2508323 , 1946 ;
反应条件
sodium amide in pentane
4 h;
参考文献
Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1512 - 1519
反应条件
hydroxylamine hydrochloride; sodium carbonate in methanol; water
0.166667 h; Ambient temperature;
参考文献
Sedova. V. F.; Shkurko, O. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 5 p. 593 - 597
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 5 p. 694 - 699
反应条件
in dichloromethane
1 h;
参考文献
Krajewski; Les; Cybulski; Chilmonczyk; Bronowska; Szelejewska-Wozniakowska
Polish Journal of Chemistry, 2001 , vol. 75, # 1 p. 71 - 78
反应条件
in dichloromethane
T=5°C; 0.5 h;
参考文献
Raw, Steven A.
Tetrahedron Letters, 2009 , vol. 50, # 8 p. 946 - 948
反应条件
dihydrogen peroxide; sodium amide in diethyl ether
参考文献
Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1512 - 1519